Cutting-Edge Instrumentation

Cutting-Edge Instrumentation

Precision tools powering advanced research, innovation, and structural characterization.

At the heart of the Hephaestus Laboratory lies an unparalleled infrastructure. Representing a strategic investment in scientific excellence, our facility houses an impressive array of specialized equipment designed for rigorous physical, chemical, and structural analysis. Explore our state-of-the-art instruments, meticulously maintained to bridge the gap between theoretical research and real-world industrial applications.

Optical tensiometer / contact angle meter — Theta Lite, Biolin Scientific

Instrument for measuring the wettability and surface energy of solid materials through static and dynamic contact angle analysis. A controlled liquid droplet is deposited on a sample surface, and high-resolution imaging software calculates the angle formed at the solid–liquid–air interface. The system is useful for evaluating surface treatments, coatings, adhesion behavior, hydrophobicity/hydrophilicity, pharmaceutical coatings, cosmetic formulations, and material–liquid interactions. Automated dosing and image analysis improve reproducibility and allow rapid comparison of different surfaces.

ATR-FTIR spectrometer — Frontier ATR-FTIR, PerkinElmer

Fourier-transform infrared spectroscopy system equipped with attenuated total reflectance capability for rapid chemical identification of solids, liquids, polymers, organic compounds, and some inorganic materials. The ATR accessory allows direct analysis with minimal sample preparation, avoiding pellet preparation or complex pretreatment. The instrument records infrared absorption spectra that reveal characteristic molecular vibrations and functional groups. It is used for material identification, polymer characterization, pharmaceutical analysis, quality control, forensic analysis, and monitoring chemical changes in research samples.

Langmuir–Blodgett trough — KSV NIMA Langmuir-Blodgett system

Instrument for preparing controlled monolayers and multilayer ultrathin films at the air–water interface and transferring them onto solid substrates. Molecules, polymers, lipids, or nanoparticles are spread on a liquid subphase and compressed using movable barriers while surface pressure is monitored. The system enables precise control of molecular packing, surface pressure, deposition speed, and film transfer. It is used for fabricating organized thin films for nanotechnology, sensors, biomimetic coatings, organic electronics, photonics, and surface-functionalized materials.

Nitrogen adsorption porosimeter — NOVA 4200e, Quantachrome

Gas adsorption analyzer used to determine specific surface area, pore volume, and pore size distribution of porous materials. Samples are degassed and then exposed to nitrogen at liquid nitrogen temperature to generate adsorption and desorption isotherms. The resulting data can be analyzed using BET theory for surface area and BJH or DFT methods for pore size distribution. The system is suitable for catalysts, activated carbons, ceramics, rocks, cements, pharmaceuticals, battery materials, and other porous solids. Its multi-station configuration allows several samples to be analyzed efficiently.

Scanning Electron Microscope — JEOL 6300LV, JEOL

Low-vacuum scanning electron microscope used for high-resolution imaging of sample surfaces and microstructures. A focused electron beam scans the sample, producing signals that reveal surface morphology, texture, particle size, shape, and compositional contrast. The low-vacuum mode allows analysis of non-conductive or partially hydrated samples with reduced charging, while high-vacuum mode supports high-resolution imaging. The SEM is widely used in materials science, geology, biology, electronics, failure analysis, and industrial quality control. It can also support elemental analysis when coupled with EDX.

Spinning drop interfacial tension meter — SITE100, Krüss

Instrument for measuring very low interfacial tension between two immiscible liquids using the spinning drop method. A droplet of one liquid is introduced into a capillary filled with another liquid and rotated at high speed. Centrifugal forces elongate the droplet, and imaging software analyzes its shape to calculate interfacial tension. The system is particularly useful for surfactant systems, emulsions, microemulsions, enhanced oil recovery studies, pharmaceutical formulations, cosmetics, and food emulsions where ultra-low interfacial tension values are important.

Transmission Electron Microscope — JEOL TEM system, JEOL

High-resolution electron microscope used to examine thin samples at microstructural, nanostructural, and atomic scales. A high-energy electron beam is transmitted through an ultrathin specimen, producing images, diffraction patterns, and analytical signals. TEM enables observation of crystal lattices, nanoparticles, defects, interfaces, phases, and biological ultrastructure. It can be combined with techniques such as electron diffraction, EDX, and EELS for structural and compositional analysis. It is essential for advanced materials science, nanotechnology, chemistry, biology, and semiconductor research.

X-ray diffractometer — D8 FOCUS, Bruker

X-ray diffraction system used to determine crystallographic structure, phase composition, lattice parameters, and crystallite size of materials. Powdered samples are exposed to X-rays, and the diffracted intensity is recorded as a function of angle to generate a diffractogram. Peaks in the diffraction pattern correspond to crystal planes and are used for phase identification and structural analysis. The Bruker D8 FOCUS includes a vertical θ/θ goniometer and LynxEye detector for sensitive and rapid data acquisition. It is widely used in materials science, chemistry, mineralogy, pharmaceuticals, and quality control.

Poremaster Automated Mercury Porosimeter

This advanced mercury intrusion system provides high-resolution analysis of pore size distribution, total pore volume, and macroscopic porosity in solid and powder samples. By applying highly controlled pressure, it enables precise structural characterization, which is essential for advanced research in materials science, nanotechnology, and environmental engineering.

High-resolution scanning probe microscope used for nanoscale surface characterization. It produces three-dimensional topographical maps of materials by scanning the surface with a sharp cantilever tip. The system supports different imaging modes, including contact mode, tapping mode, and phase imaging, allowing the study of surface roughness, morphology, mechanical properties, adhesion, and nanoscale texture. It is suitable for polymers, biomaterials, metals, semiconductors, coatings, nanostructures, and biological samples. Its closed-loop scanning and vibration isolation improve image stability and measurement precision.

Specialized analytical system combining gas chromatography with combustion isotope ratio mass spectrometry for compound-specific stable isotope analysis. Organic compounds are first separated by GC, converted into simple gases through combustion, and then analyzed by IRMS to determine isotopic ratios such as carbon, nitrogen, oxygen, or hydrogen isotope signatures. The system is valuable for environmental studies, geochemistry, food authenticity, biogeochemical tracing, hydrocarbon source identification, ecological studies, and tracking transformation pathways of organic substances.

Hybrid analytical technique that combines the separation power of gas chromatography with the molecular identification capability of FTIR spectroscopy. Volatile components in a mixture are separated in the GC column and then transferred to an FTIR detection cell, where their infrared spectra are recorded. This enables identification of individual compounds based on their molecular fingerprints. GC-FTIR is particularly useful for complex mixtures, environmental pollutants, forensic samples, flavors, fragrances, pharmaceutical impurities, and organic compound identification where structural information is required in addition to chromatographic separation.

High-performance distributed computing and storage infrastructure designed to share computational resources across networked systems. The facility operates as a WLCG Tier Two site and supports large-scale scientific data processing, storage, and analysis. It is connected to the Worldwide LHC Computing Grid framework and supports computationally intensive research activities, particularly those requiring distributed processing and large data management. The center has operated in collaboration with CERN through a memorandum of understanding for LHC Computing GRID deployment and exploitation.

Gravimetric gas sorption analyzer used to measure adsorption and desorption of gases by materials under controlled pressure and temperature. The system uses a highly sensitive microbalance to detect small mass changes as gases interact with powders, pellets, films, porous solids, catalysts, carbons, zeolites, MOFs, and energy-storage materials. It provides adsorption–desorption isotherms and enables evaluation of gas uptake, surface area, pore characteristics, sorption kinetics, and material performance for applications such as CO₂ capture, hydrogen storage, catalysis, and porous material characterization.

Non-destructive X-ray imaging system that produces high-resolution three-dimensional reconstructions of internal structures. Samples are scanned from multiple angles while X-ray projections are collected and reconstructed into volumetric datasets. The system is suitable for biological specimens, small animals, porous materials, composites, foams, bones, organs, and industrial samples. It allows internal morphology, density variation, porosity, structural defects, and anatomical features to be studied without sectioning or destroying the sample. Dedicated software supports reconstruction, visualization, and quantitative analysis.

Instrument for measuring nanoparticle size distribution and concentration in liquid suspensions by tracking Brownian motion. Particles are illuminated by a laser and visualized through a microscope-camera system; software tracks individual particle movement and calculates hydrodynamic diameter using the Stokes–Einstein equation. The system is useful for nanoparticles, vesicles, emulsions, viruses, protein aggregates, drug delivery systems, environmental nanomaterials, and colloidal dispersions. It provides both visual confirmation and quantitative particle concentration data.

Laboratory system for measuring the permeability or hydraulic conductivity of porous materials. Samples such as soils, sands, granular materials, or other porous media are placed in a cylindrical cell, and fluid is passed through under controlled pressure conditions. The system can perform constant-head and falling-head permeability tests while recording pressure and flow data. It is useful for geotechnical engineering, hydrology, environmental studies, soil remediation, irrigation studies, and porous material research, providing information on how easily fluids move through a sample.

Analytical platform for large-scale identification and quantification of proteins in biological samples. Proteins are extracted, digested into peptides, separated by liquid chromatography, and analyzed by tandem mass spectrometry. The resulting spectra are matched to protein databases using bioinformatics tools to identify proteins, quantify abundance, and investigate post-translational modifications or biological pathways. Proteomics is used in biomedical research, biomarker discovery, pharmacology, agriculture, environmental biology, and systems biology to understand cellular function and disease mechanisms.

SAXS system for studying nanoscale structures, size distributions, shapes, and organization in materials. A stable X-ray beam from the Genix source interacts with the sample, and scattered X-rays at small angles are collected by the Pilatus 3R 300K detector. The technique is suitable for polymers, colloids, nanoparticles, proteins, gels, composites, and nanostructured materials. SAXS provides structural information in the nanometer range without requiring crystallinity, making it valuable for soft matter, biomaterials, and advanced materials research.